Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051218\ Data File : VX001676.D Acq On : 12 May 2018 19:22 Operator : JC/MD Sample : J2885-02 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 19 Sample Multiplier: 1 Quant Time: May 14 13:51:07 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 261836 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 353442 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 309732 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 162068 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 209697 55.72 ug/l 0.00 Spiked Amount 50.000 Recovery = 111.44% 35) Dibromofluoromethane 5.51 113 169644 53.96 ug/l 0.00 Spiked Amount 50.000 Recovery = 107.92% 50) Toluene-d8 8.72 98 592931 51.67 ug/l 0.00 Spiked Amount 50.000 Recovery = 103.34% 62) 4-Bromofluorobenzene 11.14 95 187584 42.58 ug/l 0.00 Spiked Amount 50.000 Recovery = 85.16% Target Compounds Qvalue -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed