Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051218\ Data File : VX001677.D Acq On : 12 May 2018 19:49 Operator : JC/MD Sample : J2885-01 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 20 Sample Multiplier: 1 Quant Time: May 14 07:23:53 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 258767 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 349318 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 304087 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 157723 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 211717 56.92 ug/l 0.00 Spiked Amount 50.000 Recovery = 113.84% 35) Dibromofluoromethane 5.51 113 169616 54.59 ug/l 0.00 Spiked Amount 50.000 Recovery = 109.18% 50) Toluene-d8 8.72 98 590146 52.03 ug/l 0.00 Spiked Amount 50.000 Recovery = 104.06% 62) 4-Bromofluorobenzene 11.14 95 187914 43.16 ug/l 0.00 Spiked Amount 50.000 Recovery = 86.32% Target Compounds Qvalue 27) cis-1,2-Dichloroethene 4.60 96 5097 1.50 ug/l 96 44) Trichloroethene 7.22 130 19595 4.94 ug/l 97 64) Tetrachloroethene 9.34 164 14546 3.43 ug/l 98 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed