No Name Entered Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\Data\VX051218\ Data File : VX001685.D Acq On : 12 May 2018 23:48 Operator : JC/MD Sample : PB109200ZHE#01 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 29 Sample Multiplier: 1 Quant Time: May 14 07:31:30 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 267440 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 370029 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 326039 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 177609 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 178314 46.39 ug/l 0.00 Spiked Amount 50.000 Recovery = 92.78% 35) Dibromofluoromethane 5.51 113 142885 43.41 ug/l 0.00 Spiked Amount 50.000 Recovery = 86.82% 50) Toluene-d8 8.72 98 513910 42.78 ug/l 0.00 Spiked Amount 50.000 Recovery = 85.56% 62) 4-Bromofluorobenzene 11.14 95 164114 35.58 ug/l 0.00 Spiked Amount 50.000 Recovery = 71.16% Target Compounds Qvalue 16) Acetone 2.45 43 6631 3.80 ug/l 100 18) Methyl Acetate 2.78 43 21709 4.73 ug/l 100 20) Methylene Chloride 2.86 84 2525 0.73 ug/l # 93 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed 82X050518W.M Thu May 31 14:08:59 2018