No Name Entered Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\Data\VX051218\ Data File : VX001687.D Acq On : 13 May 2018 00:41 Operator : JC/MD Sample : PB109200ZHE#03 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 31 Sample Multiplier: 1 Quant Time: May 14 07:38:06 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 272890 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 365926 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 324046 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 175143 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 176539 45.01 ug/l 0.00 Spiked Amount 50.000 Recovery = 90.02% 35) Dibromofluoromethane 5.51 113 142497 43.78 ug/l 0.00 Spiked Amount 50.000 Recovery = 87.56% 50) Toluene-d8 8.72 98 512763 43.16 ug/l 0.00 Spiked Amount 50.000 Recovery = 86.32% 62) 4-Bromofluorobenzene 11.14 95 163526 35.85 ug/l 0.00 Spiked Amount 50.000 Recovery = 71.70% Target Compounds Qvalue 16) Acetone 2.45 43 7097 3.98 ug/l 97 18) Methyl Acetate 2.78 43 23062 4.93 ug/l 100 20) Methylene Chloride 2.86 84 3695 1.05 ug/l 96 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed 82X050518W.M Fri Jun 01 12:19:34 2018