No Name Entered Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\Data\VX051218\ Data File : VX001688.D Acq On : 13 May 2018 01:08 Operator : JC/MD Sample : PB109200ZHE#04 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 32 Sample Multiplier: 1 Quant Time: May 14 07:42:06 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 274025 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 372498 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 329314 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 175320 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 181491 46.08 ug/l 0.00 Spiked Amount 50.000 Recovery = 92.16% 35) Dibromofluoromethane 5.51 113 144710 43.68 ug/l 0.00 Spiked Amount 50.000 Recovery = 87.36% 50) Toluene-d8 8.72 98 517967 42.83 ug/l 0.00 Spiked Amount 50.000 Recovery = 85.66% 62) 4-Bromofluorobenzene 11.14 95 165450 35.64 ug/l 0.00 Spiked Amount 50.000 Recovery = 71.28% Target Compounds Qvalue 16) Acetone 2.45 43 7606 4.25 ug/l 93 18) Methyl Acetate 2.78 43 22883 4.87 ug/l 97 20) Methylene Chloride 2.86 84 2701 0.76 ug/l 97 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed 82X050518W.M Fri Jun 01 12:19:41 2018