No Name Entered Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\Data\VX051218\ Data File : VX001689.D Acq On : 13 May 2018 01:34 Operator : JC/MD Sample : PB109200ZHE#05 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 33 Sample Multiplier: 1 Quant Time: May 14 07:46:17 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 273039 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 369445 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 322929 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 171808 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 180214 45.92 ug/l 0.00 Spiked Amount 50.000 Recovery = 91.84% 35) Dibromofluoromethane 5.51 113 143630 43.71 ug/l 0.00 Spiked Amount 50.000 Recovery = 87.42% 50) Toluene-d8 8.72 98 511669 42.66 ug/l 0.00 Spiked Amount 50.000 Recovery = 85.32% 62) 4-Bromofluorobenzene 11.14 95 162233 35.23 ug/l 0.00 Spiked Amount 50.000 Recovery = 70.46% Target Compounds Qvalue 16) Acetone 2.45 43 7722 4.33 ug/l 95 18) Methyl Acetate 2.78 43 23271 4.97 ug/l 100 20) Methylene Chloride 2.86 84 2761 0.78 ug/l 96 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed 82X050518W.M Fri Jun 01 12:19:48 2018