Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051218\ Data File : VX001690.D Acq On : 13 May 2018 02:01 Operator : JC/MD Sample : PB109200ZHE#06 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 34 Sample Multiplier: 1 Quant Time: May 14 07:47:02 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 270035 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 368846 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 321216 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 174991 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 177642 45.77 ug/l 0.00 Spiked Amount 50.000 Recovery = 91.54% 35) Dibromofluoromethane 5.51 113 143477 43.73 ug/l 0.00 Spiked Amount 50.000 Recovery = 87.46% 50) Toluene-d8 8.72 98 507958 42.42 ug/l 0.00 Spiked Amount 50.000 Recovery = 84.84% 62) 4-Bromofluorobenzene 11.14 95 160602 34.93 ug/l 0.00 Spiked Amount 50.000 Recovery = 69.86% Target Compounds Qvalue 16) Acetone 2.45 43 7018 3.98 ug/l 98 18) Methyl Acetate 2.78 43 23545 5.08 ug/l 100 20) Methylene Chloride 2.87 84 2475 0.71 ug/l # 91 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed