Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051218\ Data File : VX001692.D Acq On : 13 May 2018 02:54 Operator : JC/MD Sample : PB109200ZHE#08 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 36 Sample Multiplier: 1 Quant Time: May 14 07:49:28 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 269699 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 367415 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 324138 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 173438 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 178332 46.00 ug/l 0.00 Spiked Amount 50.000 Recovery = 92.00% 35) Dibromofluoromethane 5.51 113 142857 43.71 ug/l 0.00 Spiked Amount 50.000 Recovery = 87.42% 50) Toluene-d8 8.72 98 510493 42.79 ug/l 0.00 Spiked Amount 50.000 Recovery = 85.58% 62) 4-Bromofluorobenzene 11.14 95 161224 35.21 ug/l 0.00 Spiked Amount 50.000 Recovery = 70.42% Target Compounds Qvalue 16) Acetone 2.45 43 7328 4.16 ug/l 92 18) Methyl Acetate 2.78 43 23302 5.04 ug/l 97 20) Methylene Chloride 2.86 84 2412 0.69 ug/l 95 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed