Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051218\ Data File : VX001693.D Acq On : 13 May 2018 03:20 Operator : JC/MD Sample : PB109200ZHE#09 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 37 Sample Multiplier: 1 Quant Time: May 14 07:51:13 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 275012 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 371911 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 333364 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 181202 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 180043 45.55 ug/l 0.00 Spiked Amount 50.000 Recovery = 91.10% 35) Dibromofluoromethane 5.51 113 143407 43.35 ug/l 0.00 Spiked Amount 50.000 Recovery = 86.70% 50) Toluene-d8 8.72 98 521638 43.20 ug/l 0.00 Spiked Amount 50.000 Recovery = 86.40% 62) 4-Bromofluorobenzene 11.14 95 166686 35.96 ug/l 0.00 Spiked Amount 50.000 Recovery = 71.92% Target Compounds Qvalue 16) Acetone 2.45 43 7619 4.24 ug/l 97 18) Methyl Acetate 2.78 43 23482 4.98 ug/l 100 20) Methylene Chloride 2.86 84 2642 0.74 ug/l 88 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed