Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051218\ Data File : VX001695.D Acq On : 13 May 2018 04:13 Operator : JC/MD Sample : PB109200ZHE#11 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 39 Sample Multiplier: 1 Quant Time: May 14 07:53:06 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 270767 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 367026 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 327008 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 177554 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 178447 45.85 ug/l 0.00 Spiked Amount 50.000 Recovery = 91.70% 35) Dibromofluoromethane 5.51 113 144187 44.17 ug/l 0.00 Spiked Amount 50.000 Recovery = 88.34% 50) Toluene-d8 8.72 98 517648 43.44 ug/l 0.00 Spiked Amount 50.000 Recovery = 86.88% 62) 4-Bromofluorobenzene 11.14 95 162890 35.61 ug/l 0.00 Spiked Amount 50.000 Recovery = 71.22% Target Compounds Qvalue 16) Acetone 2.45 43 7401 4.19 ug/l 99 18) Methyl Acetate 2.78 43 22572 4.86 ug/l 99 20) Methylene Chloride 2.86 84 3032 0.87 ug/l 97 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed