Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051218\ Data File : VX001697.D Acq On : 13 May 2018 05:06 Operator : JC/MD Sample : PB109200ZHE#13 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 41 Sample Multiplier: 1 Quant Time: May 14 07:55:40 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 272530 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 371487 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 327078 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 175094 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 179431 45.81 ug/l 0.00 Spiked Amount 50.000 Recovery = 91.62% 35) Dibromofluoromethane 5.51 113 145402 44.00 ug/l 0.00 Spiked Amount 50.000 Recovery = 88.00% 50) Toluene-d8 8.72 98 516858 42.85 ug/l 0.00 Spiked Amount 50.000 Recovery = 85.70% 62) 4-Bromofluorobenzene 11.14 95 162665 35.13 ug/l 0.00 Spiked Amount 50.000 Recovery = 70.26% Target Compounds Qvalue 16) Acetone 2.45 43 7568 4.25 ug/l 99 18) Methyl Acetate 2.78 43 23318 4.99 ug/l 99 20) Methylene Chloride 2.86 84 2489 0.71 ug/l 96 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed