Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051218\ Data File : VX001699.D Acq On : 13 May 2018 05:59 Operator : JC/MD Sample : PB109200ZHE#15 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 43 Sample Multiplier: 1 Quant Time: May 14 07:58:35 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 276060 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 378206 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 336115 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 186970 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 183515 46.25 ug/l 0.00 Spiked Amount 50.000 Recovery = 92.50% 35) Dibromofluoromethane 5.51 113 147812 43.94 ug/l 0.00 Spiked Amount 50.000 Recovery = 87.88% 50) Toluene-d8 8.72 98 529874 43.15 ug/l 0.00 Spiked Amount 50.000 Recovery = 86.30% 62) 4-Bromofluorobenzene 11.14 95 169400 35.94 ug/l 0.00 Spiked Amount 50.000 Recovery = 71.88% Target Compounds Qvalue 16) Acetone 2.45 43 7486 4.15 ug/l 97 18) Methyl Acetate 2.78 43 23529 4.97 ug/l 100 20) Methylene Chloride 2.87 84 2285 0.64 ug/l 94 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed