Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051218\ Data File : VX001700.D Acq On : 13 May 2018 06:26 Operator : JC/MD Sample : PB109200ZHE#16 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 44 Sample Multiplier: 1 Quant Time: May 14 07:59:26 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 276143 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 375755 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 327297 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 174562 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 182811 46.06 ug/l 0.00 Spiked Amount 50.000 Recovery = 92.12% 35) Dibromofluoromethane 5.51 113 147088 44.01 ug/l 0.00 Spiked Amount 50.000 Recovery = 88.02% 50) Toluene-d8 8.72 98 524686 43.01 ug/l 0.00 Spiked Amount 50.000 Recovery = 86.02% 62) 4-Bromofluorobenzene 11.14 95 163365 34.88 ug/l 0.00 Spiked Amount 50.000 Recovery = 69.76% Target Compounds Qvalue 16) Acetone 2.45 43 7375 4.09 ug/l 96 18) Methyl Acetate 2.78 43 23124 4.88 ug/l 97 20) Methylene Chloride 2.86 84 2758 0.77 ug/l 96 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed