Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051218\ Data File : VX001701.D Acq On : 13 May 2018 06:52 Operator : JC/MD Sample : PB109200ZHE#17 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 45 Sample Multiplier: 1 Quant Time: May 14 08:00:59 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 278029 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 378800 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 332628 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 180378 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 183876 46.01 ug/l 0.00 Spiked Amount 50.000 Recovery = 92.02% 35) Dibromofluoromethane 5.51 113 147046 43.64 ug/l 0.00 Spiked Amount 50.000 Recovery = 87.28% 50) Toluene-d8 8.72 98 530099 43.10 ug/l 0.00 Spiked Amount 50.000 Recovery = 86.20% 62) 4-Bromofluorobenzene 11.14 95 165083 34.97 ug/l 0.00 Spiked Amount 50.000 Recovery = 69.94% Target Compounds Qvalue 16) Acetone 2.45 43 7666 4.22 ug/l 99 18) Methyl Acetate 2.78 43 22878 4.80 ug/l 99 20) Methylene Chloride 2.86 84 3171 0.88 ug/l # 96 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed