Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051218\ Data File : VX001702.D Acq On : 13 May 2018 07:19 Operator : JC/MD Sample : PB109200ZHE#18 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 46 Sample Multiplier: 1 Quant Time: May 14 08:01:43 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 272580 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 372211 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 327960 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 176441 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 180632 46.10 ug/l 0.00 Spiked Amount 50.000 Recovery = 92.20% 35) Dibromofluoromethane 5.51 113 145664 44.00 ug/l 0.00 Spiked Amount 50.000 Recovery = 88.00% 50) Toluene-d8 8.72 98 521991 43.19 ug/l 0.00 Spiked Amount 50.000 Recovery = 86.38% 62) 4-Bromofluorobenzene 11.14 95 164078 35.37 ug/l 0.00 Spiked Amount 50.000 Recovery = 70.74% Target Compounds Qvalue 16) Acetone 2.45 43 7541 4.24 ug/l 99 18) Methyl Acetate 2.78 43 23006 4.92 ug/l 100 20) Methylene Chloride 2.86 84 2413 0.69 ug/l # 88 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed