Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051218\ Data File : VX001704.D Acq On : 13 May 2018 08:12 Operator : JC/MD Sample : PB109200ZHE#20 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 48 Sample Multiplier: 1 Quant Time: May 14 08:04:08 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 275711 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 373351 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 328230 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 178727 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 181344 45.76 ug/l 0.00 Spiked Amount 50.000 Recovery = 91.52% 35) Dibromofluoromethane 5.51 113 146654 44.16 ug/l 0.00 Spiked Amount 50.000 Recovery = 88.32% 50) Toluene-d8 8.72 98 523280 43.17 ug/l 0.00 Spiked Amount 50.000 Recovery = 86.34% 62) 4-Bromofluorobenzene 11.14 95 165762 35.62 ug/l 0.00 Spiked Amount 50.000 Recovery = 71.24% Target Compounds Qvalue 16) Acetone 2.45 43 7431 4.13 ug/l 99 18) Methyl Acetate 2.78 43 22792 4.82 ug/l 98 20) Methylene Chloride 2.86 84 2760 0.77 ug/l 89 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed