Quantitation Report (LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051518\ Data File : VX001730.D Acq On : 15 May 2018 00:57 Operator : JC/MD Sample : J2856-02 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 27 Sample Multiplier: 1 Quant Time: May 16 10:59:21 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 280906 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 379557 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 341383 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 211783 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 174129 46.25 ug/l 0.00 Spiked Amount 50.000 Recovery = 92.50% 35) Dibromofluoromethane 5.51 113 143052 44.66 ug/l 0.00 Spiked Amount 50.000 Recovery = 89.32% 50) Toluene-d8 8.72 98 527618 45.99 ug/l 0.00 Spiked Amount 50.000 Recovery = 91.98% 62) 4-Bromofluorobenzene 11.14 95 181108 43.85 ug/l 0.00 Spiked Amount 50.000 Recovery = 87.70% Target Compounds Qvalue -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed