Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051518\ Data File : VX001738.D Acq On : 15 May 2018 12:00 Operator : JC/MD Sample : J2737-07DL 10X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 5 Sample Multiplier: 1 Quant Time: May 16 04:34:05 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 275618 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 368488 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 305688 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 159538 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 193602 52.40 ug/l 0.00 Spiked Amount 50.000 Recovery = 104.80% 35) Dibromofluoromethane 5.51 113 160940 51.75 ug/l 0.00 Spiked Amount 50.000 Recovery = 103.50% 50) Toluene-d8 8.72 98 570610 51.23 ug/l 0.00 Spiked Amount 50.000 Recovery = 102.46% 62) 4-Bromofluorobenzene 11.15 95 173807 43.34 ug/l 0.00 Spiked Amount 50.000 Recovery = 86.68% Target Compounds Qvalue 4) Vinyl Chloride 1.40 62 9563 2.96 ug/l 98 27) cis-1,2-Dichloroethene 4.60 96 143438 42.00 ug/l 91 44) Trichloroethene 7.22 130 60261 15.53 ug/l 100 64) Tetrachloroethene 9.34 164 410429 103.14 ug/l 98 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed