Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051518\ Data File : VX001739.D Acq On : 15 May 2018 12:27 Operator : JC/MD Sample : J2737-08 10X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 6 Sample Multiplier: 1 Quant Time: May 16 04:44:00 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 269553 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 362419 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 299736 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 155556 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 194494 53.83 ug/l 0.00 Spiked Amount 50.000 Recovery = 107.66% 35) Dibromofluoromethane 5.51 113 160266 52.40 ug/l 0.00 Spiked Amount 50.000 Recovery = 104.80% 50) Toluene-d8 8.72 98 570772 52.11 ug/l 0.00 Spiked Amount 50.000 Recovery = 104.22% 62) 4-Bromofluorobenzene 11.14 95 171634 43.52 ug/l 0.00 Spiked Amount 50.000 Recovery = 87.04% Target Compounds Qvalue 4) Vinyl Chloride 1.40 62 131078 41.493 ug/l 99 21) trans-1,2-Dichloroethene 3.17 96 6870 2.341 ug/l 92 27) cis-1,2-Dichloroethene 4.60 96 1163833 348.477 ug/l 90 44) Trichloroethene 7.22 130 645297 169.137 ug/l 100 64) Tetrachloroethene 9.34 164 162964 41.765 ug/l 98 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed