Quantitation Report (LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051518\ Data File : VX001741.D Acq On : 15 May 2018 13:21 Operator : JC/MD Sample : J2737-10 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 8 Sample Multiplier: 1 Quant Time: May 16 11:08:17 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 267719 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 358446 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 292335 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 148994 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.08 65 190020 52.95 ug/l 0.00 Spiked Amount 50.000 Recovery = 105.90% 35) Dibromofluoromethane 5.51 113 156168 51.63 ug/l 0.00 Spiked Amount 50.000 Recovery = 103.26% 50) Toluene-d8 8.72 98 551437 50.90 ug/l 0.00 Spiked Amount 50.000 Recovery = 101.80% 62) 4-Bromofluorobenzene 11.15 95 164204 42.10 ug/l 0.00 Spiked Amount 50.000 Recovery = 84.20% Target Compounds Qvalue -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed