Quantitation Report (LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051518\ Data File : VX001743.D Acq On : 15 May 2018 14:14 Operator : JC/MD Sample : J2737-03 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 10 Sample Multiplier: 1 Quant Time: May 16 04:56:39 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 264034 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 347940 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 297450 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 156616 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 189549 53.56 ug/l 0.00 Spiked Amount 50.000 Recovery = 107.12% 35) Dibromofluoromethane 5.51 113 156601 53.33 ug/l 0.00 Spiked Amount 50.000 Recovery = 106.66% 50) Toluene-d8 8.72 98 531055 50.50 ug/l 0.00 Spiked Amount 50.000 Recovery = 101.00% 62) 4-Bromofluorobenzene 11.14 95 171741 45.36 ug/l 0.00 Spiked Amount 50.000 Recovery = 90.72% Target Compounds Qvalue 4) Vinyl Chloride 1.40 62 1137 0.37 ug/l 91 21) trans-1,2-Dichloroethene 3.17 96 1676 0.58 ug/l 93 27) cis-1,2-Dichloroethene 4.60 96 62199 19.01 ug/l 93 44) Trichloroethene 7.22 130 36825 10.05 ug/l 98 64) Tetrachloroethene 9.34 164 543463 140.35 ug/l 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed