Quantitation Report (LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051518\ Data File : VX001745.D Acq On : 15 May 2018 15:08 Operator : JC/MD Sample : J2737-05 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 12 Sample Multiplier: 1 Quant Time: May 16 05:09:07 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 249369 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 337282 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 281487 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 147391 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 190075 56.87 ug/l 0.00 Spiked Amount 50.000 Recovery = 113.74% 35) Dibromofluoromethane 5.51 113 152901 53.72 ug/l 0.00 Spiked Amount 50.000 Recovery = 107.44% 50) Toluene-d8 8.72 98 513984 50.42 ug/l 0.00 Spiked Amount 50.000 Recovery = 100.84% 62) 4-Bromofluorobenzene 11.14 95 165370 45.05 ug/l 0.00 Spiked Amount 50.000 Recovery = 90.10% Target Compounds Qvalue 16) Acetone 2.45 43 1882 1.43 ug/l # 86 21) trans-1,2-Dichloroethene 3.17 96 1216 0.45 ug/l 84 27) cis-1,2-Dichloroethene 4.60 96 48773 15.79 ug/l 94 40) Benzene 6.15 78 13282 1.16 ug/l 97 52) Toluene 8.79 92 1892 0.26 ug/l 90 64) Tetrachloroethene 9.34 164 1840 0.50 ug/l # 84 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed