Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051518\ Data File : VX001747.D Acq On : 15 May 2018 16:02 Operator : JC/MD Sample : J2737-09 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 14 Sample Multiplier: 1 Quant Time: May 16 05:22:05 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 243565 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 325298 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 276607 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 142869 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.08 65 176141 53.95 ug/l 0.00 Spiked Amount 50.000 Recovery = 107.90% 35) Dibromofluoromethane 5.51 113 144017 52.46 ug/l 0.00 Spiked Amount 50.000 Recovery = 104.92% 50) Toluene-d8 8.72 98 479518 48.77 ug/l 0.00 Spiked Amount 50.000 Recovery = 97.54% 62) 4-Bromofluorobenzene 11.15 95 153373 43.33 ug/l 0.00 Spiked Amount 50.000 Recovery = 86.66% Target Compounds Qvalue 27) cis-1,2-Dichloroethene 4.60 96 6652 2.20 ug/l 84 44) Trichloroethene 7.22 130 3610 1.05 ug/l 95 64) Tetrachloroethene 9.34 164 24454 6.79 ug/l 98 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed