Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051518\ Data File : VX001748.D Acq On : 15 May 2018 16:29 Operator : JC/MD Sample : J2856-06 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 15 Sample Multiplier: 1 Quant Time: May 16 11:26:23 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 251839 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 337722 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 288438 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 149806 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 161844 47.95 ug/l 0.00 Spiked Amount 50.000 Recovery = 95.90% 35) Dibromofluoromethane 5.51 113 132405 46.46 ug/l 0.00 Spiked Amount 50.000 Recovery = 92.92% 50) Toluene-d8 8.72 98 441643 43.27 ug/l 0.00 Spiked Amount 50.000 Recovery = 86.54% 62) 4-Bromofluorobenzene 11.15 95 141047 38.38 ug/l 0.00 Spiked Amount 50.000 Recovery = 76.76% Target Compounds Qvalue -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed