Quantitation Report (LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051518\ Data File : VX001749.D Acq On : 15 May 2018 16:55 Operator : JC/MD Sample : J2737-01 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 16 Sample Multiplier: 1 Quant Time: May 16 05:26:49 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 238348 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 320166 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 261288 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 129290 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.08 65 180779 56.59 ug/l 0.00 Spiked Amount 50.000 Recovery = 113.18% 35) Dibromofluoromethane 5.51 113 146239 54.12 ug/l 0.00 Spiked Amount 50.000 Recovery = 108.24% 50) Toluene-d8 8.72 98 488615 50.49 ug/l 0.00 Spiked Amount 50.000 Recovery = 100.98% 62) 4-Bromofluorobenzene 11.15 95 148242 42.55 ug/l 0.00 Spiked Amount 50.000 Recovery = 85.10% Target Compounds Qvalue 27) cis-1,2-Dichloroethene 4.60 96 6477 2.19 ug/l 86 44) Trichloroethene 7.22 130 2969 0.88 ug/l 94 64) Tetrachloroethene 9.34 164 23182 6.82 ug/l 96 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed