Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051518\ Data File : VX001751.D Acq On : 15 May 2018 17:49 Operator : JC/MD Sample : J2737-08DL 100X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 18 Sample Multiplier: 1 Quant Time: May 16 05:31:48 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 243224 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 320223 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 261861 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 119623 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 173136 53.11 ug/l 0.00 Spiked Amount 50.000 Recovery = 106.22% 35) Dibromofluoromethane 5.51 113 143214 53.00 ug/l 0.00 Spiked Amount 50.000 Recovery = 106.00% 50) Toluene-d8 8.72 98 481035 49.70 ug/l 0.00 Spiked Amount 50.000 Recovery = 99.40% 62) 4-Bromofluorobenzene 11.15 95 143854 41.28 ug/l 0.00 Spiked Amount 50.000 Recovery = 82.56% Target Compounds Qvalue 4) Vinyl Chloride 1.40 62 12530 4.40 ug/l 99 27) cis-1,2-Dichloroethene 4.60 96 103360 34.30 ug/l 92 44) Trichloroethene 7.22 130 57087 16.93 ug/l 98 64) Tetrachloroethene 9.34 164 14480 4.25 ug/l 96 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed