Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051518\ Data File : VX001752.D Acq On : 15 May 2018 18:16 Operator : JC/MD Sample : J2796-01 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 19 Sample Multiplier: 1 Quant Time: May 16 05:35:06 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 241818 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 322162 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 262337 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 128212 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.08 65 182108 56.18 ug/l 0.00 Spiked Amount 50.000 Recovery = 112.36% 35) Dibromofluoromethane 5.51 113 149355 54.94 ug/l 0.00 Spiked Amount 50.000 Recovery = 109.88% 50) Toluene-d8 8.72 98 497318 51.07 ug/l 0.00 Spiked Amount 50.000 Recovery = 102.14% 62) 4-Bromofluorobenzene 11.15 95 150656 42.97 ug/l 0.00 Spiked Amount 50.000 Recovery = 85.94% Target Compounds Qvalue 16) Acetone 2.45 43 16071 12.62 ug/l 94 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed