Quantitation Report (LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051518\ Data File : VX001753.D Acq On : 15 May 2018 18:43 Operator : JC/MD Sample : J2796-02 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 20 Sample Multiplier: 1 Quant Time: May 16 11:46:08 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 241122 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 323338 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 272082 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 141982 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 178233 55.15 ug/l 0.00 Spiked Amount 50.000 Recovery = 110.30% 35) Dibromofluoromethane 5.51 113 147543 54.07 ug/l 0.00 Spiked Amount 50.000 Recovery = 108.14% 50) Toluene-d8 8.72 98 493115 50.46 ug/l 0.00 Spiked Amount 50.000 Recovery = 100.92% 62) 4-Bromofluorobenzene 11.15 95 156481 44.47 ug/l 0.00 Spiked Amount 50.000 Recovery = 88.94% Target Compounds Qvalue 4) Vinyl Chloride 1.40 62 2251 0.80 ug/l # 86 27) cis-1,2-Dichloroethene 4.60 96 198022 66.28 ug/l 91 29) Tetrahydrofuran 5.18 42 5422 4.28 ug/l 98 44) Trichloroethene 7.22 130 27084 7.96 ug/l 99 64) Tetrachloroethene 9.34 164 39299 11.10 ug/l 96 65) Chlorobenzene 10.15 112 3482 0.47 ug/l 91 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed