Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051518\ Data File : VX001755.D Acq On : 15 May 2018 19:37 Operator : JC/MD Sample : J2796-04 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 22 Sample Multiplier: 1 Quant Time: May 16 05:44:43 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 237681 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 317337 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 259595 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 127038 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 179949 56.48 ug/l 0.00 Spiked Amount 50.000 Recovery = 112.96% 35) Dibromofluoromethane 5.51 113 149629 55.87 ug/l 0.00 Spiked Amount 50.000 Recovery = 111.74% 50) Toluene-d8 8.72 98 487304 50.81 ug/l 0.00 Spiked Amount 50.000 Recovery = 101.62% 62) 4-Bromofluorobenzene 11.15 95 149175 43.20 ug/l 0.00 Spiked Amount 50.000 Recovery = 86.40% Target Compounds Qvalue 16) Acetone 2.45 43 10439 8.34 ug/l 96 27) cis-1,2-Dichloroethene 4.60 96 8557 2.91 ug/l 91 64) Tetrachloroethene 9.35 164 1663 0.49 ug/l # 78 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed