Quantitation Report (LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051518\ Data File : VX001757.D Acq On : 15 May 2018 20:31 Operator : JC/MD Sample : J2737-07 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 24 Sample Multiplier: 1 Quant Time: May 16 04:30:10 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 237256 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 316823 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 271631 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 139289 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 173032 54.41 ug/l 0.00 Spiked Amount 50.000 Recovery = 108.82% 35) Dibromofluoromethane 5.51 113 144010 53.86 ug/l 0.00 Spiked Amount 50.000 Recovery = 107.72% 50) Toluene-d8 8.72 98 486688 50.82 ug/l 0.00 Spiked Amount 50.000 Recovery = 101.64% 62) 4-Bromofluorobenzene 11.15 95 153046 44.39 ug/l 0.00 Spiked Amount 50.000 Recovery = 88.78% Target Compounds Qvalue 4) Vinyl Chloride 1.40 62 35859 12.90 ug/l 100 12) 1,1-Dichloroethene 2.38 96 2595 1.11 ug/l 96 21) trans-1,2-Dichloroethene 3.17 96 4625 1.79 ug/l 91 27) cis-1,2-Dichloroethene 4.60 96 988721 336.34 ug/l 90 40) Benzene 6.14 78 2558 0.24 ug/l 99 44) Trichloroethene 7.22 130 336434 100.87 ug/l 99 64) Tetrachloroethene 9.35 164 4199894 1187.73 ug/l 98 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed