Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051718\ Data File : VX001783.D Acq On : 17 May 2018 11:46 Operator : JC/MD Sample : VX0517WBL01 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 3 Sample Multiplier: 1 Quant Time: May 18 04:23:41 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 376554 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 503153 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 412415 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 232049 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 267558 53.01 ug/l 0.00 Spiked Amount 50.000 Recovery = 106.02% 35) Dibromofluoromethane 5.51 113 226025 53.23 ug/l 0.00 Spiked Amount 50.000 Recovery = 106.46% 50) Toluene-d8 8.72 98 823113 54.13 ug/l 0.00 Spiked Amount 50.000 Recovery = 108.26% 62) 4-Bromofluorobenzene 11.14 95 249156 45.50 ug/l 0.00 Spiked Amount 50.000 Recovery = 91.00% Target Compounds Qvalue -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed