Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051718\ Data File : VX001786.D Acq On : 17 May 2018 13:19 Operator : JC/MD Sample : J2853-03 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 6 Sample Multiplier: 1 Quant Time: May 18 04:29:27 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 300627 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 398091 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 331926 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 172229 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 211089 52.39 ug/l 0.00 Spiked Amount 50.000 Recovery = 104.78% 35) Dibromofluoromethane 5.51 113 180191 53.64 ug/l 0.00 Spiked Amount 50.000 Recovery = 107.28% 50) Toluene-d8 8.72 98 628705 52.25 ug/l 0.00 Spiked Amount 50.000 Recovery = 104.50% 62) 4-Bromofluorobenzene 11.15 95 186746 43.11 ug/l 0.00 Spiked Amount 50.000 Recovery = 86.22% Target Compounds Qvalue 21) trans-1,2-Dichloroethene 3.17 96 1696 0.52 ug/l 89 27) cis-1,2-Dichloroethene 4.60 96 92368 24.80 ug/l 90 44) Trichloroethene 7.22 130 57553 13.73 ug/l 97 64) Tetrachloroethene 9.34 164 1409097 326.11 ug/l 97 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed