Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051718\ Data File : VX001787.D Acq On : 17 May 2018 13:46 Operator : JC/MD Sample : J2853-07 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 7 Sample Multiplier: 1 Quant Time: May 18 04:32:05 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 299585 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 402545 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 316967 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 162748 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 215000 53.54 ug/l 0.00 Spiked Amount 50.000 Recovery = 107.08% 35) Dibromofluoromethane 5.51 113 183507 54.02 ug/l 0.00 Spiked Amount 50.000 Recovery = 108.04% 50) Toluene-d8 8.72 98 632089 51.95 ug/l 0.00 Spiked Amount 50.000 Recovery = 103.90% 62) 4-Bromofluorobenzene 11.14 95 180751 41.26 ug/l 0.00 Spiked Amount 50.000 Recovery = 82.52% Target Compounds Qvalue 4) Vinyl Chloride 1.40 62 108966 31.04 ug/l 99 12) 1,1-Dichloroethene 2.38 96 3537 1.19 ug/l 92 21) trans-1,2-Dichloroethene 3.17 96 11042 3.39 ug/l 93 27) cis-1,2-Dichloroethene 4.60 96 2274038 612.64 ug/l 89 44) Trichloroethene 7.22 130 3487 0.82 ug/l 97 64) Tetrachloroethene 9.34 164 7344 1.78 ug/l 97 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed