Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051718\ Data File : VX001788.D Acq On : 17 May 2018 14:13 Operator : JC/MD Sample : J2853-08 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 8 Sample Multiplier: 1 Quant Time: May 18 04:33:21 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 291911 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 396757 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 315507 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 155194 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 211089 53.95 ug/l 0.00 Spiked Amount 50.000 Recovery = 107.90% 35) Dibromofluoromethane 5.51 113 179386 53.58 ug/l 0.00 Spiked Amount 50.000 Recovery = 107.16% 50) Toluene-d8 8.72 98 623287 51.98 ug/l 0.00 Spiked Amount 50.000 Recovery = 103.96% 62) 4-Bromofluorobenzene 11.14 95 175825 40.72 ug/l 0.00 Spiked Amount 50.000 Recovery = 81.44% Target Compounds Qvalue 21) trans-1,2-Dichloroethene 3.15 96 1082 0.34 ug/l # 79 27) cis-1,2-Dichloroethene 4.60 96 320821 88.70 ug/l 90 44) Trichloroethene 7.22 130 434232 103.96 ug/l 97 64) Tetrachloroethene 9.34 164 832893 202.79 ug/l 98 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed