Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051718\ Data File : VX001789.D Acq On : 17 May 2018 14:39 Operator : JC/MD Sample : J2853-11 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 9 Sample Multiplier: 1 Quant Time: May 18 04:34:44 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 294003 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 397444 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 320087 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 159836 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 207706 52.71 ug/l 0.00 Spiked Amount 50.000 Recovery = 105.42% 35) Dibromofluoromethane 5.51 113 177884 53.04 ug/l 0.00 Spiked Amount 50.000 Recovery = 106.08% 50) Toluene-d8 8.72 98 623182 51.88 ug/l 0.00 Spiked Amount 50.000 Recovery = 103.76% 62) 4-Bromofluorobenzene 11.14 95 178840 41.35 ug/l 0.00 Spiked Amount 50.000 Recovery = 82.70% Target Compounds Qvalue 9) 1,1,2-Trichlorotrifluoroet 2.39 101 2554 0.85 ug/l 95 21) trans-1,2-Dichloroethene 3.16 96 791 0.25 ug/l # 78 27) cis-1,2-Dichloroethene 4.60 96 66418 18.23 ug/l 92 30) Chloroform 5.21 83 1420 0.24 ug/l 97 44) Trichloroethene 7.22 130 17074 4.08 ug/l 93 64) Tetrachloroethene 9.34 164 272271 65.34 ug/l 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed