Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051718\ Data File : VX001792.D Acq On : 17 May 2018 15:59 Operator : JC/MD Sample : J2853-15 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 12 Sample Multiplier: 1 Quant Time: May 18 04:37:57 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 296536 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 393495 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 314668 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 163700 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 205786 51.77 ug/l 0.00 Spiked Amount 50.000 Recovery = 103.54% 35) Dibromofluoromethane 5.51 113 176361 53.11 ug/l 0.00 Spiked Amount 50.000 Recovery = 106.22% 50) Toluene-d8 8.72 98 614613 51.68 ug/l 0.00 Spiked Amount 50.000 Recovery = 103.36% 62) 4-Bromofluorobenzene 11.14 95 179003 41.80 ug/l 0.00 Spiked Amount 50.000 Recovery = 83.60% Target Compounds Qvalue 9) 1,1,2-Trichlorotrifluoroet 2.39 101 2673 0.88 ug/l 99 17) Carbon Disulfide 2.57 76 3111 0.41 ug/l # 87 21) trans-1,2-Dichloroethene 3.17 96 1383 0.43 ug/l # 84 27) cis-1,2-Dichloroethene 4.60 96 64940 17.68 ug/l 90 30) Chloroform 5.21 83 1524 0.25 ug/l 96 44) Trichloroethene 7.22 130 15444 3.73 ug/l 98 64) Tetrachloroethene 9.34 164 273729 66.82 ug/l 97 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed