Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051718\ Data File : VX001793.D Acq On : 17 May 2018 16:26 Operator : JC/MD Sample : J2853-16 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 13 Sample Multiplier: 1 Quant Time: May 18 04:39:46 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 296438 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 399492 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 316171 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 164738 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 215091 54.13 ug/l 0.00 Spiked Amount 50.000 Recovery = 108.26% 35) Dibromofluoromethane 5.51 113 183509 54.43 ug/l 0.00 Spiked Amount 50.000 Recovery = 108.86% 50) Toluene-d8 8.72 98 645744 53.48 ug/l 0.00 Spiked Amount 50.000 Recovery = 106.96% 62) 4-Bromofluorobenzene 11.14 95 191947 44.15 ug/l 0.00 Spiked Amount 50.000 Recovery = 88.30% Target Compounds Qvalue 4) Vinyl Chloride 1.40 62 6116 1.76 ug/l 100 27) cis-1,2-Dichloroethene 4.60 96 7004 1.91 ug/l 92 64) Tetrachloroethene 9.34 164 1666 0.40 ug/l 95 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed