Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051718\ Data File : VX001794.D Acq On : 17 May 2018 16:53 Operator : JC/MD Sample : J2853-17 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 14 Sample Multiplier: 1 Quant Time: May 18 04:41:04 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 282953 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 381932 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 305898 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 154140 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 193905 51.13 ug/l 0.00 Spiked Amount 50.000 Recovery = 102.26% 35) Dibromofluoromethane 5.51 113 167169 51.87 ug/l 0.00 Spiked Amount 50.000 Recovery = 103.74% 50) Toluene-d8 8.72 98 588833 51.01 ug/l 0.00 Spiked Amount 50.000 Recovery = 102.02% 62) 4-Bromofluorobenzene 11.14 95 168599 40.56 ug/l 0.00 Spiked Amount 50.000 Recovery = 81.12% Target Compounds Qvalue 4) Vinyl Chloride 1.41 62 1132 0.34 ug/l # 71 12) 1,1-Dichloroethene 2.38 96 1003 0.36 ug/l # 75 21) trans-1,2-Dichloroethene 3.17 96 2232 0.72 ug/l 92 27) cis-1,2-Dichloroethene 4.60 96 501470 143.04 ug/l 89 30) Chloroform 5.23 83 1321 0.23 ug/l # 82 44) Trichloroethene 7.22 130 394298 98.07 ug/l 100 64) Tetrachloroethene 9.34 164 1604950 403.04 ug/l 98 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed