Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051718\ Data File : VX001795.D Acq On : 17 May 2018 17:20 Operator : JC/MD Sample : J2853-18 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 15 Sample Multiplier: 1 Quant Time: May 18 04:42:46 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 279040 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 378673 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 303484 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 155162 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.08 65 214148 57.26 ug/l 0.00 Spiked Amount 50.000 Recovery = 114.52% 35) Dibromofluoromethane 5.51 113 182809 57.21 ug/l 0.00 Spiked Amount 50.000 Recovery = 114.42% 50) Toluene-d8 8.72 98 635915 55.56 ug/l 0.00 Spiked Amount 50.000 Recovery = 111.12% 62) 4-Bromofluorobenzene 11.14 95 183257 44.47 ug/l 0.00 Spiked Amount 50.000 Recovery = 88.94% Target Compounds Qvalue 4) Vinyl Chloride 1.40 62 92102 28.16 ug/l 99 27) cis-1,2-Dichloroethene 4.60 96 37029 10.71 ug/l 91 64) Tetrachloroethene 9.34 164 7262 1.84 ug/l 96 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed