Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051718\ Data File : VX001796.D Acq On : 17 May 2018 17:47 Operator : JC/MD Sample : J2853-12 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 16 Sample Multiplier: 1 Quant Time: May 18 04:47:14 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 283524 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 380931 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 303139 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 154867 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 202722 53.34 ug/l 0.00 Spiked Amount 50.000 Recovery = 106.68% 35) Dibromofluoromethane 5.51 113 174385 54.25 ug/l 0.00 Spiked Amount 50.000 Recovery = 108.50% 50) Toluene-d8 8.72 98 604319 52.49 ug/l 0.00 Spiked Amount 50.000 Recovery = 104.98% 62) 4-Bromofluorobenzene 11.14 95 177240 42.76 ug/l 0.00 Spiked Amount 50.000 Recovery = 85.52% Target Compounds Qvalue 4) Vinyl Chloride 1.40 62 6355 1.91 ug/l 97 12) 1,1-Dichloroethene 2.37 96 721 0.26 ug/l # 70 21) trans-1,2-Dichloroethene 3.17 96 5495 1.78 ug/l 96 27) cis-1,2-Dichloroethene 4.60 96 1594570 453.92 ug/l 89 44) Trichloroethene 7.22 130 56300 14.04 ug/l 98 64) Tetrachloroethene 9.34 164 393695 99.77 ug/l 98 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed