Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051718\ Data File : VX001797.D Acq On : 17 May 2018 18:13 Operator : JC/MD Sample : J2853-14 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 17 Sample Multiplier: 1 Quant Time: May 18 04:51:28 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 275071 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 367071 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 279738 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 126574 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 195317 52.97 ug/l 0.00 Spiked Amount 50.000 Recovery = 105.94% 35) Dibromofluoromethane 5.51 113 167541 54.08 ug/l 0.00 Spiked Amount 50.000 Recovery = 108.16% 50) Toluene-d8 8.72 98 566012 51.02 ug/l 0.00 Spiked Amount 50.000 Recovery = 102.04% 62) 4-Bromofluorobenzene 11.15 95 155936 39.04 ug/l 0.00 Spiked Amount 50.000 Recovery = 78.08% Target Compounds Qvalue 4) Vinyl Chloride 1.40 62 712 0.22 ug/l # 80 21) trans-1,2-Dichloroethene 3.17 96 837 0.28 ug/l # 83 24) 1,1-Dichloroethane 3.70 63 2111 0.40 ug/l # 86 27) cis-1,2-Dichloroethene 4.60 96 80351 23.58 ug/l 91 30) Chloroform 5.21 83 1564 0.28 ug/l # 77 44) Trichloroethene 7.22 130 16327 4.23 ug/l 98 64) Tetrachloroethene 9.34 164 9822 2.70 ug/l 98 65) Chlorobenzene 10.15 112 1949 0.25 ug/l 89 91) 1,2-Dichlorobenzene 12.40 146 5457 1.21 ug/l 100 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed