Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051718\ Data File : VX001798.D Acq On : 17 May 2018 18:40 Operator : JC/MD Sample : J2853-03DL 4X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 18 Sample Multiplier: 1 Quant Time: May 18 04:53:07 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 259105 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 346103 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 270785 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 124544 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 156216 44.98 ug/l 0.00 Spiked Amount 50.000 Recovery = 89.96% 35) Dibromofluoromethane 5.51 113 132504 45.37 ug/l 0.00 Spiked Amount 50.000 Recovery = 90.74% 50) Toluene-d8 8.72 98 454989 43.49 ug/l 0.00 Spiked Amount 50.000 Recovery = 86.98% 62) 4-Bromofluorobenzene 11.15 95 125653 33.36 ug/l 0.00 Spiked Amount 50.000 Recovery = 66.72% Target Compounds Qvalue 27) cis-1,2-Dichloroethene 4.60 96 19480 6.07 ug/l 96 44) Trichloroethene 7.22 130 13115 3.60 ug/l 99 64) Tetrachloroethene 9.34 164 359705 102.04 ug/l 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed