Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051718\ Data File : VX001800.D Acq On : 17 May 2018 19:34 Operator : JC/MD Sample : J2853-08DL 4X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 20 Sample Multiplier: 1 Quant Time: May 18 04:57:02 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 257238 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 344857 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 273134 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 137896 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 154989 44.95 ug/l 0.00 Spiked Amount 50.000 Recovery = 89.90% 35) Dibromofluoromethane 5.51 113 134293 46.14 ug/l 0.00 Spiked Amount 50.000 Recovery = 92.28% 50) Toluene-d8 8.72 98 456678 43.81 ug/l 0.00 Spiked Amount 50.000 Recovery = 87.62% 62) 4-Bromofluorobenzene 11.14 95 130808 34.86 ug/l 0.00 Spiked Amount 50.000 Recovery = 69.72% Target Compounds Qvalue 27) cis-1,2-Dichloroethene 4.60 96 78504 24.63 ug/l 91 44) Trichloroethene 7.22 130 116264 32.03 ug/l 100 64) Tetrachloroethene 9.34 164 248018 69.75 ug/l 98 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed