Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX051718\ Data File : VX001801.D Acq On : 17 May 2018 20:01 Operator : JC/MD Sample : J2853-11 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 21 Sample Multiplier: 1 Quant Time: May 18 04:58:18 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 316231 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 444623 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 371435 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 200345 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 237002 55.91 ug/l 0.00 Spiked Amount 50.000 Recovery = 111.82% 35) Dibromofluoromethane 5.51 113 200492 53.43 ug/l 0.00 Spiked Amount 50.000 Recovery = 106.86% 50) Toluene-d8 8.72 98 701063 52.17 ug/l 0.00 Spiked Amount 50.000 Recovery = 104.34% 62) 4-Bromofluorobenzene 11.15 95 210628 43.53 ug/l 0.00 Spiked Amount 50.000 Recovery = 87.06% Target Compounds Qvalue 9) 1,1,2-Trichlorotrifluoroet 2.39 101 3245 1.00 ug/l 98 27) cis-1,2-Dichloroethene 4.60 96 65778 16.79 ug/l 91 44) Trichloroethene 7.22 130 17464 3.73 ug/l 100 64) Tetrachloroethene 9.34 164 323555 66.92 ug/l 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed