Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052218\ Data File : VX001894.D Acq On : 22 May 2018 15:36 Operator : JC/MD Sample : J2988-08 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 5 Sample Multiplier: 1 Quant Time: May 24 11:41:42 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 325492 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 464230 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 403137 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 216932 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 256864 58.88 ug/l 0.00 Spiked Amount 50.000 Recovery = 117.76% 35) Dibromofluoromethane 5.51 113 206581 52.73 ug/l 0.00 Spiked Amount 50.000 Recovery = 105.46% 50) Toluene-d8 8.72 98 737764 52.58 ug/l 0.00 Spiked Amount 50.000 Recovery = 105.16% 62) 4-Bromofluorobenzene 11.14 95 236359 46.79 ug/l 0.00 Spiked Amount 50.000 Recovery = 93.58% Target Compounds Qvalue -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed