Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052218\ Data File : VX001895.D Acq On : 22 May 2018 16:03 Operator : JC/MD Sample : J2988-01 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 6 Sample Multiplier: 1 Quant Time: May 23 08:10:34 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 324878 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 460294 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 408666 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 218785 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 256063 58.80 ug/l 0.00 Spiked Amount 50.000 Recovery = 117.60% 35) Dibromofluoromethane 5.51 113 205216 52.83 ug/l 0.00 Spiked Amount 50.000 Recovery = 105.66% 50) Toluene-d8 8.72 98 718828 51.67 ug/l 0.00 Spiked Amount 50.000 Recovery = 103.34% 62) 4-Bromofluorobenzene 11.14 95 233738 46.66 ug/l 0.00 Spiked Amount 50.000 Recovery = 93.32% Target Compounds Qvalue 27) cis-1,2-Dichloroethene 4.60 96 12880 3.20 ug/l 96 44) Trichloroethene 7.21 130 13287 2.74 ug/l 98 64) Tetrachloroethene 9.34 164 86604 16.28 ug/l 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed