Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052218\ Data File : VX001896.D Acq On : 22 May 2018 16:30 Operator : JC/MD Sample : J2988-05 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 7 Sample Multiplier: 1 Quant Time: May 23 08:11:55 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 319026 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 448273 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 400744 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 217911 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 248361 58.08 ug/l 0.00 Spiked Amount 50.000 Recovery = 116.16% 35) Dibromofluoromethane 5.51 113 198315 52.42 ug/l 0.00 Spiked Amount 50.000 Recovery = 104.84% 50) Toluene-d8 8.72 98 699183 51.60 ug/l 0.00 Spiked Amount 50.000 Recovery = 103.20% 62) 4-Bromofluorobenzene 11.14 95 227019 46.54 ug/l 0.00 Spiked Amount 50.000 Recovery = 93.08% Target Compounds Qvalue 16) Acetone 2.45 43 2607 1.55 ug/l 100 27) cis-1,2-Dichloroethene 4.60 96 12273 3.10 ug/l 98 44) Trichloroethene 7.22 130 8339 1.77 ug/l 100 64) Tetrachloroethene 9.34 164 309602 59.35 ug/l 98 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed