Quantitation Report (LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052218\ Data File : VX001897.D Acq On : 22 May 2018 16:56 Operator : JC/MD Sample : J2988-07 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 8 Sample Multiplier: 1 Quant Time: May 23 04:19:32 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 318051 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 451579 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 396427 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 212140 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 245587 57.61 ug/l 0.00 Spiked Amount 50.000 Recovery = 115.22% 35) Dibromofluoromethane 5.51 113 196262 51.50 ug/l 0.00 Spiked Amount 50.000 Recovery = 103.00% 50) Toluene-d8 8.72 98 675743 49.51 ug/l 0.00 Spiked Amount 50.000 Recovery = 99.02% 62) 4-Bromofluorobenzene 11.14 95 220539 44.88 ug/l 0.00 Spiked Amount 50.000 Recovery = 89.76% Target Compounds Qvalue 4) Vinyl Chloride 1.40 62 5202 1.40 ug/l 100 16) Acetone 2.45 43 4006 2.39 ug/l 93 27) cis-1,2-Dichloroethene 4.60 96 39568 10.04 ug/l 95 64) Tetrachloroethene 9.34 164 1131 0.22 ug/l # 72 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed