Quantitation Report (LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052218\ Data File : VX001898.D Acq On : 22 May 2018 17:23 Operator : JC/MD Sample : J2988-02RE Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 9 Sample Multiplier: 1 Quant Time: May 23 08:18:32 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 304957 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 439273 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 391169 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 204605 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 251668 61.57 ug/l 0.00 Spiked Amount 50.000 Recovery = 123.14% 35) Dibromofluoromethane 5.51 113 199985 53.95 ug/l 0.00 Spiked Amount 50.000 Recovery = 107.90% 50) Toluene-d8 8.72 98 700436 52.76 ug/l 0.00 Spiked Amount 50.000 Recovery = 105.52% 62) 4-Bromofluorobenzene 11.14 95 223505 46.75 ug/l 0.00 Spiked Amount 50.000 Recovery = 93.50% Target Compounds Qvalue 16) Acetone 2.45 43 3693 2.30 ug/l 99 27) cis-1,2-Dichloroethene 4.61 96 6451 1.71 ug/l 83 44) Trichloroethene 7.22 130 9418 2.04 ug/l 95 64) Tetrachloroethene 9.34 164 54816 10.76 ug/l 97 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed