Quantitation Report    (QT Reviewed)

  Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052218\
  Data File : VX001902.D                                          
  Acq On    : 22 May 2018  19:10
  Operator  : JC/MD
  Sample    : PB109525TB
  Misc      : 5.0mL/MSVOA_X/WATER
  ALS Vial  : 13   Sample Multiplier: 1

  Quant Time: May 23 04:10:53 2018
  Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M
  Quant Title  : SW846 8260
  QLast Update : Tue May 15 01:36:22 2018
  Response via : Initial Calibration

   Internal Standards                R.T. QIon  Response  Conc Units Dev(Min)
   --------------------------------------------------------------------------
     1) Pentafluorobenzene           5.67  168   213155    50.00 ug/l    0.00
    34) 1,4-Difluorobenzene          6.87  114   289663    50.00 ug/l    0.00
    63) Chlorobenzene-d5            10.12  117   231295    50.00 ug/l    0.00
    72) 1,4-Dichlorobenzene-d4      12.09  152   101339    50.00 ug/l    0.00

   System Monitoring Compounds                                        
    33) 1,2-Dichloroethane-d4        6.07   65   136823    47.89 ug/l    0.00  
     Spiked Amount     50.000                      Recovery   =   95.78%
    35) Dibromofluoromethane         5.51  113   113674    46.50 ug/l    0.00  
     Spiked Amount     50.000                      Recovery   =   93.00%
    50) Toluene-d8                   8.72   98   392094    44.79 ug/l    0.00  
     Spiked Amount     50.000                      Recovery   =   89.58%
    62) 4-Bromofluorobenzene        11.14   95   108755    34.50 ug/l    0.00  
     Spiked Amount     50.000                      Recovery   =   69.00%

   Target Compounds                                                   Qvalue
    16) Acetone                      2.45   43     7674     6.84 ug/l      91
    18) Methyl Acetate               2.78   43    23809     7.26 ug/l      96
    20) Methylene Chloride           2.86   84     7871     3.28 ug/l      96
    68) m/p-Xylenes                 10.37  106      960     0.24 ug/l      93
   --------------------------------------------------------------------------

   (#) = qualifier out of range (m) = manual integration (+) = signals summed